| ¹H NMR (M/I = 10,000, Papp = 9.4 W, soluble fraction, CDCl₃) | Trans: 84.1 ± 3.1 %; Cis: 15.8 ± 3.1 % |
|---|---|
| ¹H NMR (M/I = 35,000, Papp = 2.6 W, soluble fraction, CDCl₃) | Trans: 30.3 ± 1.4 %; Cis: 69.7 ± 1.4 % |
| DSC (Papp = 2.6 W) | Crystalline melting temperature was not observed |
| DSC (Papp = 9.4 W) | Tm = 42.5 ± 0.6 °C |
| ¹H NMR spectra and DSC curves | Image data were not transcribed |
Andrew Vogler, Arfa Abrar Malik, Diego M. Alzate-Sanchez. “Apparent power as a unifying metric for frontal polymerization.” ChemRxiv (). https://doi.org/10.26434/chemrxiv.15003418/v3
| ¹H NMR (M/I = 10,000), Main result | Trans-isomer: 74 % |
|---|---|
| ¹H NMR (M/I = 35,000), Main result | Trans-isomer: 72 % |
| ¹H NMR (M/I = 10,000), SI result | Trans: 26 %; Cis: 74 % |
| ¹H NMR (M/I = 35,000), SI result | Trans: 28 %; Cis: 72 % |
| ¹H NMR spectra | Image data were not transcribed |
| Gas chromatography | Major product eluting at 2.7 minutes |
|---|---|
| Mass spectrum | Signal at 2.7 min having an 89 % NIST library match with 5-ethylidene-2-norbornene |
| Gas chromatogram and mass spectrum | Image data were not transcribed |